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Publication Details
AFRICAN RESEARCH NEXUS
SHINING A SPOTLIGHT ON AFRICAN RESEARCH
One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl
2
complex
International Journal of Molecular Sciences, Volume 14, No. 12, Year 2013
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Description
[NiCl2(C14H12N2)(H2O)] complex has been synthesized from nickel chloride hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM). © 2013 by the authors; licensee MDPI, Basel, Switzerland.
Authors & Co-Authors
Barakat, Assem
Saudi Arabia, Riyadh
King Saud University
Al-Noaimi, Mousa Z.
Jordan, Zarqa
Hashemite University
Suleiman, Mohammed A.
Palestine, Nablus
An-najah National University
Al-Dwayyan, Abdullah Saleh
Saudi Arabia, Riyadh
King Saud University
Hammouti, Belkheir
Morocco, Oujda
Laboratoire de Chimie Appliquée et Environnement Lcae
Ben Hadda, Taibi
Morocco, Oujda
Université Mohammed Premier Oujda
Haddad, Salim F.
Jordan, Amman
The University of Jordan
Boshaala, Ahmed M.A.
Libya, Benghazi
University of Benghazi
Warad, I. Khaleel
Palestine, Nablus
An-najah National University
Statistics
Citations: 74
Authors: 9
Affiliations: 7
Identifiers
Doi:
10.3390/ijms141223941
ISSN:
16616596
e-ISSN:
14220067