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Publication Details
AFRICAN RESEARCH NEXUS
SHINING A SPOTLIGHT ON AFRICAN RESEARCH
chemical engineering
Simultaneous determination of pyrethroids from pesticide residues in porcine muscle and pasteurized milk using GC
Journal of Separation Science, Volume 32, No. 2, Year 2009
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Description
The principal goal of this work was to develop an efficient method for the simultaneous determination of four pyrethroid (PYR) insecticides, cyfluthrin, cyhalothrin, cypermethrin, and deltamethrin, in porcine muscle and pasteurized milk using liquid - liquid extraction (LLE). Sample extraction was carried out with and without additional column cleanup procedures, and the final determination was made using GC with electron-capture detector (ECD). The pesticide identity was confirmed using GC-MS in the SIM mode. Since there were minor differences between the extraction procedures, extraction without the additional cleanup procedure was used throughout the work. The method was validated by fortifying blank samples with half, two, and four times the maximum residue limit (MRL)of each PYR. The average recoveries (n = 6) ranged from 83.5 to 99.2% and 82.9 to 109% in porcine muscle and pasteurized milk, respectively. The repeatability of measurements expressed as RSDs, was in the range of 1.7-11.9 and 1.5-10.3% in porcine muscle and pasteurized milk, respectively. The LODs ranged from 3.3 to 9 and 3 to 8.1 ppm, whereas the LOQs ranged from 10 to 27.4 and 9 to 24.6 ppm, in porcine muscle and pasteurized milk, respectively. The applicability of the method was demonstrated by analyzing real samples collected from major cities in the Republic of Korea. No residues of the selected pesticides were detected in any of the samples. © 2009 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.
Authors & Co-Authors
Khay, Sathya
South Korea, Gwangju
Chonnam National University
Abd El-Aty, A. M.
South Korea, Seoul
Konkuk University
Egypt, Giza
Faculty of Veterinary Medicine
Choi, Jeong-Heui
South Korea, Gwangju
Chonnam National University
Shin, Eun-ho
South Korea, Gwangju
Chonnam National University
Shin, Ho-chul
South Korea, Seoul
Konkuk University
Kim, Jin-suk
South Korea, Seoul
Konkuk University
Chang, Byungjoon
South Korea, Seoul
Konkuk University
Lee, Chiho
South Korea, Seoul
Konkuk University
Shin, Sung Chul
Unknown Affiliation
Jeong, Jiyoon
Unknown Affiliation
Shim, Jae-Han
South Korea, Gwangju
Chonnam National University
Statistics
Citations: 48
Authors: 11
Affiliations: 3
Identifiers
Doi:
10.1002/jssc.200800481
ISSN:
16159306
e-ISSN:
16159314
Research Areas
Environmental